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2 article(s) from Sjödin, Martin

A versatile route to polythiophenes with functional pendant groups using alkyne chemistry

Xiao Huang,
Li Yang,
Rikard Emanuelsson,
Jonas Bergquist,
Maria Strømme,
Martin Sjödin and
Adolf Gogoll

Beilstein J. Org. Chem. 2016, 12, 2682–2688, doi:10.3762/bjoc.12.265

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Scheme 1: Previous and present EDOT functionalization routes.

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Scheme 2: The synthetic route from glycidol to pyEDOT (3).

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Scheme 3: The synthetic route from D-mannitol diketal to eEDOT 8 and TMS-eEDOT 8’.

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Scheme 4: New EDOT derivatives 9–13 accessible from pyEDOT with bromo-pendant group precursors via Sonogashir...

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Figure 1: CVs of electrochemical polymerization of (a) pyEDOT 3 and (b) EDOT in MeCN solution with 0.1 M TEAPF...

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Figure 2: CVs of electrochemical polymerization of (a) pyEDOT-DeT (9), (b) pyEDOT-AQ (12) and (c) pyEDOT-MVPF...

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Published 09 Dec 2016

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Hydroquinone–pyrrole dyads with varied linkers

Hao Huang,
Christoffer Karlsson,
Maria Strømme,
Martin Sjödin and
Adolf Gogoll

Beilstein J. Org. Chem. 2016, 12, 89–96, doi:10.3762/bjoc.12.10

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Figure 1: Structure of pyrrole/hydroquinone derivatives 3-(2,5-dimethoxyphenyl)-1H-pyrrole (1) and 3-(1,4-dih...

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Figure 2: Hydroquinone dimethyl ether functionalized pyrroles with linkers L discussed in this study.

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Scheme 1: Synthetic route for 3-(2,5-dimethoxybenzyl)-1H-pyrrole (3a). Conditions: i) Pd(PPh₃)₄, Na₂CO₃ (2 M ...

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Scheme 2: Synthetic route for 3-(2,5-dimethoxystyryl)-1H-pyrrole (3c); cis-4c and trans-4c were separated chr...

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Scheme 3: Synthesis of 3-((2,5-dimethoxyphenyl)ethynyl)-1H-pyrrole (3d). Conditions: i) Ethynyltrimethylsilan...

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Scheme 4: Synthesis of 3-(2,5-dimethoxyphenethyl)-1H-pyrrole (3b). Conditions: i) Pd/C, MeOH/acetone, rt, 1.5...

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Figure 3: ¹H NMR spectra (400 MHz, CDCl₃ solution) of the DMB-pyrrole dyads (aliphatic signals not shown).

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Figure 4: ¹³C NMR spectra (100.6 MHz, CDCl₃ solution) of the DMB-pyrrole dyads (aliphatic signals not shown).

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Figure 5: UV–vis absorption spectra of 1, 3a–d, (full lines) and the reference compounds DMB, DMB-VI, DMB-EN ...

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Figure 6: Calculated HOMO for 3a (a) and 3d (b).

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Published 18 Jan 2016

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